Test Name |
Purpose |
Type
of Test |
Duration of Test |
Comments |
ASTM C
227,
Potential alkali-reactivity of cement-aggregate combinations
(mortar-bar method) |
To test the
susceptibility of cement-aggregate combinations to expansive
reactions involving alkalies |
Mortar bars stored
over water at 37.8°C (100°F) and high relative humidity |
Varies: first
measurement at 14 days, then 1, 2, 3, 4, 6, 9, and 12 months; every
6 months after that as necessary |
Test may not produce significant expansion, especially for
carbonate aggregate. Long test duration. Expansions may not be from
ASR. |
ASTM C 289,
Potential alkali-silica reactivity of aggregates |
To determine potential reactivity of siliceous
aggregates |
Sample reacted with alkaline solution at 80°C
(176°F). |
24 hours |
Quick results. Some aggregates give low expansions even though
they have high silica content. Not reliable. |
ASTM C 294,
Constituents of natural mineral aggregates |
To give descriptive nomenclature for the more common
or important natural minerals—an aid in determining their
performance |
Visual identification |
Short duration—as long
as it takes to visually examine the sample |
These descriptions are used to characterize naturally-occurring
minerals that makeup common aggregate sources. |
ASTM C 295,
Petrographic examination of aggregates for concrete |
To outline petrographic examination procedures for
aggregates—an aid in determining their performance |
Visual and microscopic examination of prepared
samples—sieve analysis, microscopy, scratch or acid tests |
Short duration—visual examination does not involve
long test periods |
Usually includes optical microscopy. Also may include XRD
analysis, differential thermal analysis, or infrared
spectroscopy—see ASTM C 294 for descriptive nomenclature. |
ASTM C 342,
Potential volume change of cement-aggregate combinations |
To determine the potential ASR expansion of
cement-aggregate combinations |
Mortar bars stored in water at 23°C (73.4°F) |
52 weeks |
Primarily used for aggregates from Oklahoma, Kansas, Nebraska,
and Iowa. |
ASTM C 441,
Effectiveness of mineral admixtures or GBFS in preventing excessive
expansion of concrete due to alkali-silica reaction |
To determine effectiveness of supplementary cementing materials
in controlling expansion from ASR |
Mortar bars—using Pyrex glass as aggregate—stored over water at
37.8°C (100°F) and high relative humidity |
Varies: first measurement at 14 days, then 1, 2, 3, 4, 5, 9, and
12 months; every 6 months after that as necessary |
Highly reactive artificial aggregate may not represent real
aggregate conditions. Pyrex contains alkalies. |
ASTM C 856,
Petrographic examination of hardened concrete |
To outline petrographic examination procedures for hardened
concrete—useful in determining condition or performance |
Visual (unmagnified) and microscopic examination of prepared
samples |
Short duration — includes preparation of samples and visual and
microscope examination |
Specimens can be examined with stereo microscopes, polarizing
microscopes, metallographic microscopes, and scanning electron
microscope. |
ASTM C 856 (AASHTO T 299),
Annex uranyl- acetate treatment procedure |
To identify products of ASR in hardened concrete |
Staining of a freshly-exposed concrete surface and viewing under
UV light |
Immediate results |
Identifies small amounts of ASR gel whether they
cause expansion or not. Opal, a natural aggregate, and carbonated
paste can glow—interpret results accordingly. Tests must be
supplemented by petrographic examination and physical tests for
determining concrete expansion |
Los Alamos staining method (Powers 1999) |
To identify products of ASR in hardened concrete. |
Staining of a freshly-exposed concrete surface with two different
reagents. |
Immediate results |
ASTM C 1260 (AASHTOT303),
Potential alkali reactivity of aggregates (mortar-bar method) |
To test the potential for deleterious alkali-silica reaction of
aggregate in mortar bars |
Immersion of mortar bars in alkaline solution at 80°C (176°F) |
16 days |
Very fast alternative to C 227. Useful for slowly reacting
aggregates or those that produce expansion late in the reaction. |
ASTM C 1293,
Determination of length change of concrete due to alkali-silica
reaction (concrete prism test) |
To determine the potential ASR expansion of cement-aggregate
combinations. |
Concrete prisms stored over water at 38°C (100.4°F) |
Varies: first measurement at 7 days, then 28and 56 days, then
3,6,9,and 12 months; every 6 months as after that as necessary |
Requires long test duration for meaningful results. Use as a
supplement to C 227,C 295, C 289, and C 1260. Similar to CSA
A23.2-14A. |
Accelerated concrete prism test (modified ASTM C 1293) |
To determine the potential ASR expansion of cement-aggregate
combinations. |
Concrete prisms stored over water at 60°C(140°F) |
3 month (91 days) |
Fast alternative to C 227. Good correlation to ASTM C 227 for
carbonate and sedimentary rocks. |